Materials Characterization and Synthesis

Eyring Materials Center

FT-IR – Nicolet iS50 with RaptIR microscope

Description

FT-IR is a technique used to identify and analyze materials based on inter-atomic and lattice vibrations.

Capabilities – Bench

  • Built in Diamond ATR with 60lbs force
  • Optical resolution < 0.09 cm-1
  • Spectral range 11000-375 cm-1
    • Polaris IR source (9600- 10 cm-1)
    • White light source (13,000-2000 cm-1)
    • DLaTGS- KBr detector – 12,500 – 375 cm-1
    • DLaTGS-Diamond detecor (ATR module only) 11000-100cm-1 (measurement range limited to 11000-375cm-1 because of the beamsplitter)

Capabilities – Microscope

  • 5 megapixel camera and 1 cm square sample view in <20s in visible
  • 15x standard diffraction-limited objective
  • Ge-tip ATR (350 µm)
  • Automated aperture
  • LN2 cooled MCT-A high sensitivity detector (11,700-600 cm-1)
  • InGaAs NIR detector (12,000 – 3800 cm-1)
  • Automated stage up to 40mm sample thickness and 5 kg
  • up to 10 spectra/s
  • spatial resolution < 5 µm

Contact

Emmanuel Soignard
Operations Director
[email protected]
480.965.7242

Techniques

  • Optical spectroscopy

Rates

Service or materialASU rateNonprofit or academic rateNotes
Equipment use$31.00/hr$65.00/hr
Equipment use with staff assistance$91.00/hr$161.00/hr

Video

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